Carbon-13 n.m.r. spectra of large, rigid molecules recorded in 0·1 M solution of Fe(acac)3 exhibit pronounced line-broadening. The resonances of the quaternary carbon atoms can be specifically defined due to chemical elimination of long range couplings.
U. Séquin and A. I. Scott, J. Chem. Soc., Chem. Commun., 1974, 1041 DOI: 10.1039/C39740001041
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