Nucleophilic addition of 2-lithio-2-methyl-1,3-dithian to the dialdehyde (2) gives the two diastereo-isomers (3) and (7) was transformed into a new class of carbohydrate dithiepan derivatives (11)–(13).
A. Gateau-Olesker, S. D. Gero, C. Pascard-Billy, C. Riche, A. Sepulchre, G. Vass and N. A. Hughes, J. Chem. Soc., Chem. Commun., 1974, 811 DOI: 10.1039/C39740000811
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