Several ribonucleoside 3′,5′-cyclic phosphates (7b) have been prepared in good yields by the action of base on the corresponding 2′-protected 3′-diphenyl phosphates (5); thymidine 3′,5′-cyclic phosphate (7; R = H, B = thymine-1) has similarly been prepared from both thymidine 3′- and 5′-diphenyl phosphates (8a and 8b).
J. H. van Boom, P. M. J. Burgers, P. van Deursen and C. B. Reese, J. Chem. Soc., Chem. Commun., 1974, 618 DOI: 10.1039/C39740000618
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