Reaction of the dibromocarbene adduct of 4-vinylcyclohexene with methyl-lithium at –48° to –50° gives the spiro-compound (IV), but by modifying the reaction condition a ready route to the exo-tricyclo-[3,3,1,02,4] ring system is obtained.
M. S. Baird, J. Chem. Soc., Chem. Commun., 1974, 197 DOI: 10.1039/C39740000197
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