SCHEDULED MAINTENANCE
Methods were examined for the determination of small amounts of C8 to C10 alcohols in their phthalate esters involving the use of vanadium 8-hydroxyquinolinate in benzene or toluene and 3,5-dinitrobenzoyl chloride in pyridine as colorimetric reagents. Two modified procedures are presented that will reliably determine free alcohols in the 0·01 to 0·4 per cent. m/m range.
S. Harrison, H. Hinchcliffe and G. L. Woodroffe, Analyst, 1974, 99, 491 DOI: 10.1039/AN9749900491
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