Cyclohexanespiro-4′-dioxolan exists in CFCl3 preferentially in the O-axial conformation. The slight preference for O-axial is decreased in the geminally substituted 2′,2′-dimethyl derivative and increased in the corresponding 1-t-butylpiperidine-4-spiro-4′-derivatives. These variations are discussed.
R. A. Y. Jones, A. R. Katritzky, D. L. Nicol and R. Scattergood, J. Chem. Soc., Perkin Trans. 2, 1973, 337 DOI: 10.1039/P29730000337
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