Several cis- and trans-2-halogeno-3-morpholinothietan 1,1-dioxides have been synthesized. Their configurations and conformations have been assigned from 1H n.m.r. data, including lanthanide-induced shifts. The stereo-chemical assignments agree with predicted relative thermodynamic stabilities based upon inspection of molecular models.
P. Del Buttero and S. Maiorana, J. Chem. Soc., Perkin Trans. 1, 1973, 2540 DOI: 10.1039/P19730002540
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