A new one-step synthesis of alkyl 2,4,6-trioxoadamantane-1-carboxylates has resulted from the reaction of crotonoyl and methacryloyl chlorides with the pyrrolidine enamines of dialkyl 4-oxocyclohexane-1,1-dicarboxylates.
P. W. Hickmott, H. Suschitzky and R. Urbani, J. Chem. Soc., Perkin Trans. 1, 1973, 2063 DOI: 10.1039/P19730002063
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