The results of nuclear magnetic resonance, X-ray and thermal measurements on solid 2,3-dimethylbutane in the temperature range 80–160 K are reported. It is concluded that two amorphous phases and at least two crystalline phases exist in this temperature range: transitions to the crystalline state can occur from either of the amorphous phases. At 80 K the crystalline state is found to be orthorhombic with cell dimensions 12.51, 10.13 and 4.74 Å.
K. J. Anderton and J. P. Llewellyn, J. Chem. Soc., Faraday Trans. 2, 1973, 69, 1249 DOI: 10.1039/F29736901249
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