The reactions of pentacarbonyliron(0) and hexacarbonylmolybdenum(0) with thiocyanogen yield the polymeric complexes [Fe(CO)2(SCN)2] and [Mo(CO)4(SCN)2] respectively. The complexes are thermally and hydrolytically unstable, I.r. spectra are reported.
J. Granifo and H. Müller, J. Chem. Soc., Dalton Trans., 1973, 1891 DOI: 10.1039/DT9730001891
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