The equilibrium constant of complexation of bromine with hexamethylphosphoric triamide (HMPA) has been determined by 1H n.m.r. spectroscopy by using a ‘competitive complexation’ method. Solid adducts of bromine with poly-HMPA, a polymer analogue of HMPA, have been isolated from chloroform solutions.
Y. Ozari and J. Jagur-Grodzinski, J. Chem. Soc., Dalton Trans., 1973, 474 DOI: 10.1039/DT9730000474
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