The new complex [Et4N]2[W(CO)8H2] has been synthesized and its structure determined by an X-ray structural analysis; all atoms have been located (including hydrogens), the two W–H–W linkages being equivalent and symmetrical, with d(W–H)= 1·85(7)Å; ∠(W-H–W′)= 110(6)°, and ∠(H–W–H′)= 70(6)°.
M. R. Churchill, S. W.-Y. N. Chang, M. L. Berch and A. Davison, J. Chem. Soc., Chem. Commun., 1973, 691 DOI: 10.1039/C39730000691
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