Addition of Na+C5H5– and NiBr2,2C2H4(OMe)2 to [Me4N][(π-C5H5)coIII(πCB7H8)] previously reduced with sodium naphthalide formed a new bimetallic mixed metal monocarbon metallocarborane (πC5H5)CoIII(πCB7H8)NiIV(πC5H5), isolated in at least four isomeric forms, representing an extension of lthe polylhedral expansion reaction to monocarbon metallocarboranes.
C. G. Salentine and M. F. Hawthorne, J. Chem. Soc., Chem. Commun., 1973, 560 DOI: 10.1039/C39730000560
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