S-Alkylisothiourea hydrobromides are converted into S-alkyl thiocarbamates with isopentyl nitrite under mild and anhydrous conditions via nitrosoimine intermediates.
K. Akiba and N. Inamoto, J. Chem. Soc., Chem. Commun., 1973, 13a DOI: 10.1039/C3973000013A
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