The 13C n.m.r. chemical shifts of bridging and terminal carbonyl carbons in (π-C5H5)2Rh2(CO)3 have been established from 103Rh–13C coupling data at –80°; at 20° the spectrum shows rapid intramolecular interconversion of all carbonyl groups.
J. Evans, B. F. G. Johnson, J. Lewis and J. R. Norton, J. Chem. Soc., Chem. Commun., 1973, 79 DOI: 10.1039/C39730000079
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