Chlorination of 1,3,5-trithian in water-acetic acid proceeds through bischloromethyl sulphide which subsequently undergoes stepwise degradation through chloromethanesulphinyl chloride to give chloromethane-sulphonyl chloride.
J. S. Grossert and R. F. Langler, J. Chem. Soc., Chem. Commun., 1973, 49 DOI: 10.1039/C39730000049
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