Treatment of pyrene or 1-bromopyrene with limited amounts of bromine affords 1,6-dibromopyrene and 1,8-di-bromopyrene (not isolated pure by previous workers). Further bromination of either dibromide gives 1,3,6-tri-bromopyrene.
J. Grimshaw and J. Trocha-Grimshaw, J. Chem. Soc., Perkin Trans. 1, 1972, 1622 DOI: 10.1039/P19720001622
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