The long-sought ν4(a1′) mode of (PNCl2)3 has been located at 172 cm–1 in solution and its symmetry species confirmed by a Raman Study of an oriented single crystal. Experimental evidence from the crystal spectra also allowed distinction between e′ and e″ species. A reassignment of the spectrum is offered.
D. M. Adams and W. S. Fernando, J. Chem. Soc., Dalton Trans., 1972, 2503 DOI: 10.1039/DT9720002503
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