The diamagnetic, nonelectrolytic complexes M(CN)4(CNR)4(M = Mo or W; R = Me, Et, Prn, Pri, But, or CPh3) give unexpectedly simple i.r. and Raman spectra in the C–N stretching region. On the basis of X-ray data for Mo(CN)4(CNMe)4, all the complexes are presumed to have dodecahedral configurations.
R. V. Parish and P. G. Simms, J. Chem. Soc., Dalton Trans., 1972, 2389 DOI: 10.1039/DT9720002389
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