Crystals of the title compound are monoclinic, space-group P21/c, with a= 6·293(9), b= 11·444(15), c= 13·992(15)Å, β= 120·7(2)°. The structure was solved by direct methods from diffractometer data and refined by least-squares to R 0·050 for 1368 independent reflections. The molecule has a virtual mirror plane of symmetry.
C. S. Liu, S. C. Nyburg, J. T. Szymański and J. C. Thompson, J. Chem. Soc., Dalton Trans., 1972, 1129 DOI: 10.1039/DT9720001129
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