Improved methods for the preparation of complexes [WCl4L2] and the preparation of new complexes [WOCl2L3](L = tertiary phosphine or tertiary arsine) are described. The structures are assigned on the basis of i.r. and 1H and 31P n.m.r. spectroscopy. The magnetic and n.m.r. properties are discussed.
A. V. Butcher, J. Chatt, G. J. Leigh and P. L. Richards, J. Chem. Soc., Dalton Trans., 1972, 1064 DOI: 10.1039/DT9720001064
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