Coupling of Grignard reagents with bromoapopinene, prepared by treatment of apopinene with NBS, gives 4-alkylated derivatives of apopinene in high yields; of particular interest is the convenient preparation of trans-δ-pinene.
D. Joulain, C. Moreau and M. Pfau, J. Chem. Soc., Chem. Commun., 1972, 1110b DOI: 10.1039/C3972001110B
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