Hydroformylation of propene using stoicheiometric amounts of Rh4(CO)12 and hydrogen, and direct synthesis of the first acyl cluster compounds are reported; catalytic synthesis in the presence of tertiary phosphines takes place together with decomposition of the phosphine.
P. Chini, S. Martinengo and G. Garlaschelli, J. Chem. Soc., Chem. Commun., 1972, 709b DOI: 10.1039/C3972000709B
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