19 F N.m.r. spectra of [MF(PR3)3][BF4], M = Pd or Pt, unequivocally confirm the assigned structures and comparison of coupling parameters with those in isostructural hydrido-complexes suggests a very small s character for the platinum–fluorine bond.
K. R. Dixon and J. J. McFarland, J. Chem. Soc., Chem. Commun., 1972, 1274 DOI: 10.1039/C39720001274
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