A route to carbohydrate furoxan derivatives has been developed which involves treatment of a carbohydrate α-keto toluene-p-sulphonate with hydroxylamine hydrochloride in aqueous pyridine, followed by treatment of the resultant oximino-pyridinium salt with sodium nitrite.
C. S. Wu, W. A. Szarek and J. K. N. Jones, J. Chem. Soc., Chem. Commun., 1972, 1117 DOI: 10.1039/C39720001117
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