Nickel carbonyl in tetrahydrofuran reductively converts polyhalogenomethyl groups into di- or mono-halogenomethyls under quite mild conditions which permit the stereoselective synthesis of 5-bromo-lyxose and -xylose.
T. Kunieda, T. Tamura and T. Takizawa, J. Chem. Soc., Chem. Commun., 1972, 885 DOI: 10.1039/C39720000885
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