Reaction of Os3(CO)12 with PPh3 in the mole ratio of 1 : 2 gives a mixture of nine products, three of which have been defined by X-ray crystallography as HOs3(CO)9(PPh3)(PPh2C6H4), Os3(CO)8(PPh2)(Ph)(PPh-C6H4), and Os3(CO)7(PPh2)2(C6H4).
C. W. Bradford, R. S. Nyholm, G. J. Gainsford, J. M. Guss, P. R. Ireland and R. Mason, J. Chem. Soc., Chem. Commun., 1972, 87 DOI: 10.1039/C39720000087
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