A series of tungsten tetrahydrides [WH4(PR3)4](PR3= tertiary phosphine) has been prepared; the 1H n.m.r. spectra in deuteriobenzene at room temperature show metal hydride spectra consistent with a rigid structure.
B. Bell, J. Chatt, G. J. Leigh and T. Ito, J. Chem. Soc., Chem. Commun., 1972, 34 DOI: 10.1039/C39720000034
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