Decoupling of phosphorus and hydrogen nuclei in the proton n.m.r. spectra of phosphorus-containing esters has been observed upon the addition of a paramagnetic complexing agent. With increased concentrations of the complexing agent loss of all structure in the signals from the ester moieties is observed.
R. Engel and A. Jung, J. Chem. Soc. C, 1971, 1761 DOI: 10.1039/J39710001761
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