Fusion of 3-deoxyhex-2-enopyranosyl esters or the isomeric 2-hydroxyglycal esters with theophylline or 2,6-dichloropurine in the presence of an acidic catalyst affords (3′-deoxyhex-2′-enopyranosyl)purine nucleoside derivatives. Anomeric configurations can be assigned by n.m.r. methods.
R. J. Ferrier and M. M. Ponpipom, J. Chem. Soc. C, 1971, 560 DOI: 10.1039/J39710000560
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