The mass spectra of the dimeric forms of glycolaldehyde and glyceraldehyde are reported for solid samples injected directly into the source of a mass spectrometer. Both compounds fragment via routes which are explicable in terms of the isomerisation of the molecular ion via a four-membered transition state.
E. F. H. Brittain, W. O. George and G. C. S. Collins, J. Chem. Soc. B, 1971, 2414 DOI: 10.1039/J29710002414
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