The conformational analysis of saturated heterocycles. Part XXXI. 1-t-Butylpiperidine-4-spiro-4′-(1′,3′-dioxolan) and 1,3-dioxan-5-spiro-4′-(1′,3′-dioxolan)

Richard A. Y. Jones; A. R. Katritzky; P. G. Lehman; K. A. F. Record; B. B. Shapiro

doi:10.1039/J29710001302

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The conformational analysis of saturated heterocycles. Part XXXI. 1-t-Butylpiperidine-4-spiro-4′-(1′,3′-dioxolan) and 1,3-dioxan-5-spiro-4′-(1′,3′-dioxolan)

Richard A. Y. Jones, A. R. Katritzky, P. G. Lehman, K. A. F. Record and (Mrs)B. B. Shapiro

Abstract

The use of dipole moment and n.m.r. measurements of spiro-1-t-butylpiperidines and spiro-1,3-dioxans is proposed as a general method for the investigation of intramolecular interaction in situations of defined geometry. The method is applied to the title compounds.

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DOI: https://doi.org/10.1039/J29710001302
Article type: Paper

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J. Chem. Soc. B, 1971, 1302-1307

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The conformational analysis of saturated heterocycles. Part XXXI. 1-t-Butylpiperidine-4-spiro-4′-(1′,3′-dioxolan) and 1,3-dioxan-5-spiro-4′-(1′,3′-dioxolan)

R. A. Y. Jones, A. R. Katritzky, P. G. Lehman, K. A. F. Record and B. B. Shapiro, J. Chem. Soc. B, 1971, 1302 DOI: 10.1039/J29710001302

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Journal of the Chemical Society B: Physical Organic

The conformational analysis of saturated heterocycles. Part XXXI. 1-t-Butylpiperidine-4-spiro-4′-(1′,3′-dioxolan) and 1,3-dioxan-5-spiro-4′-(1′,3′-dioxolan)

Abstract

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The conformational analysis of saturated heterocycles. Part XXXI. 1-t-Butylpiperidine-4-spiro-4′-(1′,3′-dioxolan) and 1,3-dioxan-5-spiro-4′-(1′,3′-dioxolan)

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