The title compound when prepared by the reaction of pivaloyl chloride and 2-methylbut-2-ene in the presence of stannic chloride contains impurities inseparable by preparative gas chromatography. A purer product is obtained by pyrolysis of 2,2,5,5-tetramethyl-4-diazohexan-3-one.
H. N. A. Al-Jallo, B. J. Arnold, B. J. Rothwell and E. S. Waight, J. Chem. Soc. B, 1971, 846 DOI: 10.1039/J29710000846
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