A new polynuclear oxocarbonyl of osmium having the formula Os6O6(CO)16 has been isolated from the products obtained during the synthesis of Os3(CO)12. The mass and i.r. spectra of the new compound and of Os4O4(CO)12 are reported and compared.
C. W. Bradford and R. S. Nyholm, J. Chem. Soc. A, 1971, 2038 DOI: 10.1039/J19710002038
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