SCHEDULED MAINTENANCE
A voltammetric study of the complex previously formulated as [Re{S2C2(CN)2}2]22– has shown that it must be reformulated as [Re{S2C2(CN)2}2]44–, which undergoes one one-electron reduction and two one-electron oxidation processes. Oxidation of [Re{S2C2(CN)2}3]2– with iodine afforded [ReO{S2C2(CN)2}2]–, which may be reduced voltammetrically to a dianion.
N. G. Connelly, C. J. Jones and J. A. McCleverty, J. Chem. Soc. A, 1971, 712 DOI: 10.1039/J19710000712
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