X-ray analysis of (Me3CNPCl)2 establishes that the (N–P)2 ring is slightly puckered; the exocyclic P–Cl bonds are unexpectedly long; and there are significant differences in the co-ordination of the chemically equivalent nitrogen atoms.
K. W. Muir and J. F. Nixon, J. Chem. Soc. D, 1971, 1405 DOI: 10.1039/C29710001405
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