A molecular beam–mass spectrometer has been constructed and used to show that VF5 and CrF5 have monomeric vapours and the NbF5, TaF5, IrF5, and SbF5 are associated in the vapour phase.
M. J. Vasile, G. R. Jones and W. E. Falconer, J. Chem. Soc. D, 1971, 1355 DOI: 10.1039/C29710001355
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