31  P nuclear magnetic resonance study of conformers of trans-[MCl(CO)(PBu2tR)2](M = Rh or Ir; R = Me, Et, or Prn)

B. E. Mann; C. Masters; B. L. Shaw; R. E. Stainbank

doi:10.1039/C29710001103

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³¹P nuclear magnetic resonance study of conformers of trans-[MCl(CO)(PBu₂^tR)₂](M = Rh or Ir; R = Me, Et, or Prⁿ)

B. E. Mann, C. Masters, B. L. Shaw and R. E. Stainbank

Abstract

The low temperature ³¹P n.m.r. spectra of the complexes trans-[MCl(CO)(PRBu^t₂)₂](M = Rh or Ir; R = Me, Et, or Prⁿ) show the presence of three rotamers with very different chemical shifts.

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DOI: https://doi.org/10.1039/C29710001103
Article type: Paper

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J. Chem. Soc. D, 1971, 1103-1104

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³¹ P nuclear magnetic resonance study of conformers of trans-[MCl(CO)(PBu₂^tR)₂](M = Rh or Ir; R = Me, Et, or Prⁿ)

B. E. Mann, C. Masters, B. L. Shaw and R. E. Stainbank, J. Chem. Soc. D, 1971, 1103 DOI: 10.1039/C29710001103

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Journal of the Chemical Society D: Chemical Communications