An X-ray crystal structure analysis has unambiguously established the orientation and conformation of the guest molecule 2,5,5-trimethylhex-3-yn-2-ol (II) in the cage of the clathrate host 4-p-hydroxyphenyl-2,2,4-trimethylthiochroman (I).
D. D. MacNicol and F. B. Wilson, J. Chem. Soc. D, 1971, 786 DOI: 10.1039/C29710000786
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