The i.r. spectra for HX,xH2O (X = Cl, Br; x= 1–4) and evidence for the existence of the complex HCl,4H2O are reported; the spectra of the dihydrates show the presence of a very strong central hydrogen bond in H5O2+, and other spectra indicate the presence of H2O, H3O+, or H5O2+ units, consistent with X-ray crystal structures.
A. S. Gilbert and N. Sheppard, J. Chem. Soc. D, 1971, 337 DOI: 10.1039/C29710000337
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