The single-crystal X-ray structure determination of the sodium molybdenum oxide bronze, Na0.9Mo6O17 shows the existence of localized MoO4 tetrahedra closely associated with the sodium atoms in a structure which otherwise comprises ReO3-type corner-sharing MoO6 octahedral slabs.
B. M. Gatehouse and D. J. Lloyd, J. Chem. Soc. D, 1971, 13 DOI: 10.1039/C29710000013
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