Reactions of t-pentylmagnesium chloride with phosphorus trichloride have given t-pentylphosphonous dichloride and di-t-pentylphosphinous chloride, which have been used to prepare t-butyl-t-pentylphosphinic acid and di-t-pentylphosphinic acid.
P. C. Crofts and D. M. Parker, J. Chem. Soc. C, 1970, 2529 DOI: 10.1039/J39700002529
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