The conformational preferences of some 1,3,2-dioxaphosphorinans are deduced from PO·CH coupling constants, and also from a temperature variation study of the chemical shifts of 5,5-gem-dimethyl groups.
A. R. Katritzky, M. R. Nesbit, J. Michalski, Z. Tulimowski and A. Zwierzak, J. Chem. Soc. B, 1970, 140 DOI: 10.1039/J29700000140
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