Alkylthio- and arylthio-fluorophosphoranes of the types R1SPF4, R1S(R2)PF3, and R1S(R2)2PF2(R1= Me, Et, or Ph; R2= Me or Ph) are prepared in good yields by the cleavage of sulphur–silicon bonds in trimethylsilylsulphides by fluorophosphoranes. The structures of the new compounds are deduced from 19F and 31P n.m.r. data.
S. C. Peake and R. Schmutzler, J. Chem. Soc. A, 1970, 1049 DOI: 10.1039/J19700001049
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