The compounds Rh2Cl2(CO)4(II) and RhCl(CO)2(OPPh3)2(III) have been prepared from the reaction of RhCl(CO)(PPh3)2(I) with a mixture of carbon monoxide and oxygen; (III) reacts with triphenylphosphine to produce (I).
J. Kiji and J. Furukawa, J. Chem. Soc. D, 1970, 977 DOI: 10.1039/C29700000977
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