CIDNP emission signals are observed in the thermal rearrangement of benzyl toluene-p-sulphenate (1) to benzyl p-tolyl sulphoxide (2) which cannot arise as a result of the rearrangement itself; the origin of the observed emission is discussed in terms of the utilization of the CIDNP technique for the detection of paramagnetic species.
J. Jacobus, J. Chem. Soc. D, 1970, 709 DOI: 10.1039/C29700000709
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