Magnitudes and signs of indirect spin coupling constants relative to 1J(CH) > 0 were investigated by heteronuclear INDOR-technique in the series MenPF5–n(n= 1,2,3) and in [MePF5]– showing that 1J(PFa) < 0, 1J(PFe) < 0, and 1J(PC) > 0.
H. Dreeskamp, C. Schumann and R. Schmutzler, J. Chem. Soc. D, 1970, 671 DOI: 10.1039/C29700000671
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