Thermal decomposition of 2-azidophenyl 2,6-dimethylphenyl sulphide (IV; X = N3) in decalin leads to 5,11-dihydro-4-methyldibenzo[b,e][1,4]thiazepine (II)via a novel rearrangement involving a nitrene.
J. I. G. Cadogan and S. Kulik, J. Chem. Soc. D, 1970, 233 DOI: 10.1039/C29700000233
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