A total synthesis of p-acetamidophenyl β-D-glucopyranosiduronic acid is reported. The type and degree of solvation were determined from the integrated n.m.r. spectra of the compound in [2H6]dimethyl sulphoxide with and without added [2H4]acetic acid.
L. Weintraub, S. R. Oles, A. Wilson and L. Wilson, J. Chem. Soc. C, 1969, 1562 DOI: 10.1039/J39690001562
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