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The gas-phase decomposition of ethyl, isopropyl, and t-butyl isothiocyanates has been studied in the pressure range of 35–350 mm. The reaction, which has been found to be the unimolecular elimination of thiocyanic acid, is followed by a slow addition of the acid to the olefins to yield mainly the isothiocyanate expected by Markownikoff addition.
N. Barroeta, A. Maccoll and A. Fava, J. Chem. Soc. B, 1969, 347 DOI: 10.1039/J29690000347
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